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Article Dans Une Revue Geostandards and Geoanalytical Research Année : 2019

NanoSr – A New Carbonate Microanalytical Reference Material for In Situ Strontium Isotope Analysis

Résumé

The in situ measurement of Sr isotopes in carbonates by MC‐ICP‐MS is limited by the availability of suitable microanalytical reference materials (RMs), which match the samples of interest. Whereas several well‐characterised carbonate reference materials for Sr mass fractions > 1000 µg g −1 are available, there is a lack of well‐characterised carbonate microanalytical RMs with lower Sr mass fractions. Here, we present a new synthetic carbonate nanopowder RM with a Sr mass fraction of ca. 500 µg g −1 suitable for microanalytical Sr isotope research (‘NanoSr’). NanoSr was analysed by both solution‐based and in situ techniques. Element mass fractions were determined using EPMA (Ca mass fraction), as well as laser ablation and solution ICP‐MS in different laboratories. The 87 Sr/ 86 Sr ratio was determined by well‐established bulk methods for Sr isotope measurements and is 0.70756 ± 0.00003 (2 s ). The Sr isotope microhomogeneity of the material was determined by LA‐MC‐ICP‐MS, which resulted in 87 Sr/ 86 Sr ratios of 0.70753 ± 0.00007 (2 s ) and 0.70757 ± 0.00006 (2 s ), respectively, in agreement with the solution data within uncertainties. Thus, this new reference material is well suited to monitor and correct microanalytical Sr isotope measurements of low‐Sr, low‐REE carbonate samples. NanoSr is available from the corresponding author.
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Dates et versions

ird-04427086 , version 1 (31-01-2024)

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Michael Weber, Federico Lugli, Bodo Hattendorf, Denis Scholz, Regina Mertz-Kraus, et al.. NanoSr – A New Carbonate Microanalytical Reference Material for In Situ Strontium Isotope Analysis. Geostandards and Geoanalytical Research, 2019, 44 (1), pp.69-83. ⟨10.1111/ggr.12296⟩. ⟨ird-04427086⟩
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